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Beilstein J. Nanotechnol. 2022, 13, 1473–1482, doi:10.3762/bjnano.13.121
Figure 1: Flowchart for combustion solution synthesis (CSS) of LiCoO2.
Figure 2: Left: XRD patterns of LiCoO2 heated at different temperatures (450–900 °C); right: average crystall...
Figure 3: Specific surface area of LCO powders as function of the temperature during combustion solution synt...
Figure 4: SEM images of LiCoO2 heated at different temperatures (450–900 °C) at 25,000× magnification.
Figure 5: Ni3+ impurity concentration depending on the synthesis temperature.
Figure 6: EPR spectra recorded in the temperature range of 5–300 K for LCO synthesized at 900 °C.
Figure 7: Experimental and simulated spectra for samples prepared at 500 °C (a) and 900 °C (b) and recorded a...
Figure 8: Components of the g-tensor for axial (complex I) and non-axial (complex II) Ni3+ ions.
Figure 9: Percentage contribution of Ni3+(I) and Ni3+(II) depending on the synthesis temperature obtained fro...
Figure 10: Nyquist plot of LiCoO2 annealed at T = 700 °C. The insert shows frequency dependences of the real p...